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Coupling using trimethyl phosphite of 4,5-dimethoxycarbonyl- and 4,5-ditrifluoromethyl-1,3-diselenole-2-thiones unexpectedly gave only tetramethoxycarbonyl- and tetratrifluoromethyl-triselenathiafulvalene respectively, while self-coupling of 4,5-dimethyl-1,3-diselenole-2-thione provided a mixture (85) of tetramethyltetraselenafulvalene and tetramethyltriselenathiafulvalene.
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